Structures by: Hofmann A.

Total: 68

MesN3

C38H60AlN3

Drescher, ReginaLin, ShujuanHofmann, AlexanderLenczyk, CarstenKachel, StephanieKrummenacher, IvoLin, ZhenyangBraunschweig, Holger

Chemical science (2020) 11, 21 5559-5564

a=10.2360(15)Å   b=32.920(5)Å   c=10.7797(14)Å

α=90°   β=105.178(5)°   γ=90°

Tertbutylaluminol

C32H58Al2

Drescher, ReginaLin, ShujuanHofmann, AlexanderLenczyk, CarstenKachel, StephanieKrummenacher, IvoLin, ZhenyangBraunschweig, Holger

Chemical science (2020) 11, 21 5559-5564

a=8.755(4)Å   b=15.965(5)Å   c=11.067(5)Å

α=90°   β=96.64(2)°   γ=90°

DMAP_koordiniert

C36H59AlN2

Drescher, ReginaLin, ShujuanHofmann, AlexanderLenczyk, CarstenKachel, StephanieKrummenacher, IvoLin, ZhenyangBraunschweig, Holger

Chemical science (2020) 11, 21 5559-5564

a=12.957(6)Å   b=16.692(7)Å   c=15.618(6)Å

α=90°   β=96.13(2)°   γ=90°

Cp3taluminol

C29H49Al

Drescher, ReginaLin, ShujuanHofmann, AlexanderLenczyk, CarstenKachel, StephanieKrummenacher, IvoLin, ZhenyangBraunschweig, Holger

Chemical science (2020) 11, 21 5559-5564

a=9.335(4)Å   b=16.672(9)Å   c=17.185(7)Å

α=90°   β=93.88(3)°   γ=90°

TMSN3

C32H58AlNSi

Drescher, ReginaLin, ShujuanHofmann, AlexanderLenczyk, CarstenKachel, StephanieKrummenacher, IvoLin, ZhenyangBraunschweig, Holger

Chemical science (2020) 11, 21 5559-5564

a=9.601(2)Å   b=12.750(3)Å   c=13.314(2)Å

α=97.397(6)°   β=93.793(15)°   γ=94.404(7)°

Terhphenylazid

C47H62AlN3

Drescher, ReginaLin, ShujuanHofmann, AlexanderLenczyk, CarstenKachel, StephanieKrummenacher, IvoLin, ZhenyangBraunschweig, Holger

Chemical science (2020) 11, 21 5559-5564

a=19.5714(5)Å   b=14.2192(3)Å   c=14.8360(4)Å

α=90°   β=96.3970(10)°   γ=90°

C15H35B2N3Se2Si2

C15H35B2N3Se2Si2

Liu, SiyuanLégaré, Marc-AndréHofmann, AlexanderRempel, AnnaHagspiel, StephanBraunschweig, Holger

Chemical Science (2019)

a=11.500(5)Å   b=12.544(6)Å   c=16.944(7)Å

α=90°   β=109.60(2)°   γ=90°

C33H42B2N2Se2

C33H42B2N2Se2

Liu, SiyuanLégaré, Marc-AndréHofmann, AlexanderRempel, AnnaHagspiel, StephanBraunschweig, Holger

Chemical Science (2019)

a=12.9542(7)Å   b=12.1291(7)Å   c=20.4231(10)Å

α=90°   β=90.590(2)°   γ=90°

C33H42B2N2Se2.96

C33H42B2N2Se2.96

Liu, SiyuanLégaré, Marc-AndréHofmann, AlexanderRempel, AnnaHagspiel, StephanBraunschweig, Holger

Chemical Science (2019)

a=8.6416(7)Å   b=13.4779(11)Å   c=14.6575(12)Å

α=75.409(3)°   β=77.096(3)°   γ=85.540(3)°

C35H82B4N6S4Si4

C35H82B4N6S4Si4

Liu, SiyuanLégaré, Marc-AndréHofmann, AlexanderRempel, AnnaHagspiel, StephanBraunschweig, Holger

Chemical Science (2019)

a=9.1005(10)Å   b=11.8019(13)Å   c=12.4035(13)Å

α=80.466(3)°   β=84.795(3)°   γ=86.977(4)°

C33H42B2N2Te2

C33H42B2N2Te2

Liu, SiyuanLégaré, Marc-AndréHofmann, AlexanderRempel, AnnaHagspiel, StephanBraunschweig, Holger

Chemical Science (2019)

a=8.8783(8)Å   b=13.1076(11)Å   c=14.7911(13)Å

α=73.716(2)°   β=75.160(3)°   γ=83.313(2)°

C33H42B2N2S3

C33H42B2N2S3

Liu, SiyuanLégaré, Marc-AndréHofmann, AlexanderRempel, AnnaHagspiel, StephanBraunschweig, Holger

Chemical Science (2019)

a=8.4766(11)Å   b=13.3667(19)Å   c=14.6143(19)Å

α=75.204(4)°   β=77.352(4)°   γ=85.490(4)°

C30H48B2N4Se2

C30H48B2N4Se2

Liu, SiyuanLégaré, Marc-AndréHofmann, AlexanderRempel, AnnaHagspiel, StephanBraunschweig, Holger

Chemical Science (2019)

a=9.2253(4)Å   b=13.3449(5)Å   c=14.4581(6)Å

α=107.0150(10)°   β=93.8670(10)°   γ=90.0350(10)°

C34H58Al2Br2

C34H58Al2Br2

Braunschweig, HolgerKupfer, ThomasHofmann, AlexanderTröster, Tobias

Chemical Science (2019)

a=19.582(6)Å   b=8.479(2)Å   c=21.301(8)Å

α=90°   β=93.33(2)°   γ=90°

C27H44Al2Br2

C27H44Al2Br2

Braunschweig, HolgerKupfer, ThomasHofmann, AlexanderTröster, Tobias

Chemical Science (2019)

a=8.824(3)Å   b=29.234(6)Å   c=12.125(3)Å

α=90°   β=108.80(2)°   γ=90°

C46H68Al2N2

C46H68Al2N2

Braunschweig, HolgerKupfer, ThomasHofmann, AlexanderTröster, Tobias

Chemical Science (2019)

a=17.2467(17)Å   b=13.0572(9)Å   c=18.6141(16)Å

α=90°   β=90°   γ=90°

C17H29AlBr2

C17H29AlBr2

Braunschweig, HolgerKupfer, ThomasHofmann, AlexanderTröster, Tobias

Chemical Science (2019)

a=9.400(5)Å   b=14.876(9)Å   c=13.886(9)Å

α=90°   β=105.24(4)°   γ=90°

C17H29Al2Br3

C17H29Al2Br3

Braunschweig, HolgerKupfer, ThomasHofmann, AlexanderTröster, Tobias

Chemical Science (2019)

a=10.6448(18)Å   b=10.6844(20)Å   c=11.1041(12)Å

α=63.541(5)°   β=81.455(7)°   γ=73.465(6)°

C51H87Al3O3

C51H87Al3O3

Braunschweig, HolgerKupfer, ThomasHofmann, AlexanderTröster, Tobias

Chemical Science (2019)

a=14.173(9)Å   b=19.091(14)Å   c=19.858(14)Å

α=90°   β=109.37(2)°   γ=90°

C21H38Al2Cl2

C21H38Al2Cl2

Braunschweig, HolgerKupfer, ThomasHofmann, AlexanderTröster, Tobias

Chemical Science (2019)

a=9.8915(4)Å   b=21.5331(9)Å   c=11.5146(5)Å

α=90°   β=90.4570(10)°   γ=90°

C34H58Al3Br3

C34H58Al3Br3

Braunschweig, HolgerKupfer, ThomasHofmann, AlexanderTröster, Tobias

Chemical Science (2019)

a=10.1424(16)Å   b=38.371(7)Å   c=10.1825(19)Å

α=90°   β=105.719(13)°   γ=90°

Ba2 (In2 S5)

Ba2In2S5

Eisenmann, B.Hofmann, A.

Zeitschrift fuer Anorganische und Allgemeine Chemie (1990) 580, 151-159

a=13.167Å   b=12.723Å   c=11.784Å

α=90°   β=90°   γ=90°

Sr2 (Ga2 S5)

Ga2S5Sr2

Eisenmann, B.Hofmann, A.

Zeitschrift fuer Anorganische und Allgemeine Chemie (1990) 580, 151-159

a=12.523Å   b=12.034Å   c=11.18Å

α=90°   β=90°   γ=90°

Ba2 (In2 Se5)

Ba2In2Se5

Eisenmann, B.Hofmann, A.

Zeitschrift fuer Anorganische und Allgemeine Chemie (1990) 580, 151-159

a=13.657Å   b=13.182Å   c=12.225Å

α=90°   β=90°   γ=90°

C49H108B4N4Si8W2

C49H108B4N4Si8W2

Liu, SiyuanLégaré, Marc-AndréHofmann, AlexanderDellermann, TheresaBraunschweig, Holger

Chemical communications (Cambridge, England) (2020) 56, 53 7277-7280

a=12.0424(6)Å   b=8.8836(5)Å   c=31.4360(15)Å

α=90°   β=90.468(3)°   γ=90°

C20H30Al2Br2

C20H30Al2Br2

Hofmann, AlexanderLamprecht, AnnaGonzález-Belman, Oscar FDewhurst, Rian D.Jiménez-Halla, J Oscar CKachel, StephanieBraunschweig, Holger

Chemical communications (Cambridge, England) (2018) 54, 13 1639-1642

a=10.394(5)Å   b=14.012(8)Å   c=15.316(7)Å

α=90°   β=97.53(4)°   γ=90°

C32H50Al2Br2N2

C32H50Al2Br2N2

Hofmann, AlexanderLamprecht, AnnaGonzález-Belman, Oscar FDewhurst, Rian D.Jiménez-Halla, J Oscar CKachel, StephanieBraunschweig, Holger

Chemical communications (Cambridge, England) (2018) 54, 13 1639-1642

a=8.6234(20)Å   b=11.477(5)Å   c=18.064(7)Å

α=101.19(2)°   β=91.52(2)°   γ=110.23(2)°

C24H36Al2Br2

C24H36Al2Br2

Hofmann, AlexanderLamprecht, AnnaGonzález-Belman, Oscar FDewhurst, Rian D.Jiménez-Halla, J Oscar CKachel, StephanieBraunschweig, Holger

Chemical communications (Cambridge, England) (2018) 54, 13 1639-1642

a=9.136(4)Å   b=8.291(3)Å   c=16.801(8)Å

α=90°   β=101.961(15)°   γ=90°

C26H35Al2Br2N

C26H35Al2Br2N

Hofmann, AlexanderLamprecht, AnnaGonzález-Belman, Oscar FDewhurst, Rian D.Jiménez-Halla, J Oscar CKachel, StephanieBraunschweig, Holger

Chemical communications (Cambridge, England) (2018) 54, 13 1639-1642

a=8.880(6)Å   b=14.563(9)Å   c=10.658(10)Å

α=90°   β=110.01(4)°   γ=90°

Α-Glycine

C2H5NO2

Netzel, JeanetteHofmann, Andreasvan Smaalen, Sander

CrystEngComm (2008) 10, 3 335

a=5.0866Å   b=11.7731Å   c=5.4595Å

α=90°   β=111.99°   γ=90°

Na5 In Te4

InNa5Te4

Eisenmann, B.Zagler, R.Hofmann, A.

Zeitschrift fuer Naturforschung, Teil B. Anorganische Chemie, Organische Chemie (42,1987-) (1990) 45, 8-14

a=7.427Å   b=20.154Å   c=17.733Å

α=90°   β=90°   γ=90°

Na5 (In Te3)2

In2Na5Te6

Eisenmann, B.Hofmann, A.Zagler, R.

Zeitschrift fuer Naturforschung, Teil B. Anorganische Chemie, Organische Chemie (42,1987-) (1990) 45, 8-14

a=9.021Å   b=15.361Å   c=23.565Å

α=90°   β=90°   γ=90°

C16H30BNSi2W

C16H30BNSi2W

Liu, SiyuanLégaré, Marc-AndréHofmann, AlexanderDellermann, TheresaBraunschweig, Holger

Chemical communications (Cambridge, England) (2020) 56, 53 7277-7280

a=9.1544(9)Å   b=13.250(2)Å   c=17.443(3)Å

α=99.524(8)°   β=102.213(5)°   γ=106.236(4)°

C34H58Al2Br2

C34H58Al2Br2

Braunschweig, HolgerKupfer, ThomasHofmann, AlexanderTröster, Tobias

Chemical Science (2019)

a=10.367(2)Å   b=12.452(3)Å   c=15.704(3)Å

α=69.094(5)°   β=88.918(6)°   γ=67.783(5)°

C18H34B2N4S2

C18H34B2N4S2

Liu, SiyuanLégaré, Marc-AndréHofmann, AlexanderBraunschweig, Holger

Journal of the American Chemical Society (2018) 140, 36 11223-11226

a=8.0243(20)Å   b=8.053(3)Å   c=9.721(4)Å

α=105.103(9)°   β=104.95(2)°   γ=106.457(18)°

C18H34B2N4Se2

C18H34B2N4Se2

Liu, SiyuanLégaré, Marc-AndréHofmann, AlexanderBraunschweig, Holger

Journal of the American Chemical Society (2018) 140, 36 11223-11226

a=8.085(2)Å   b=8.208(3)Å   c=9.845(3)Å

α=108.77(2)°   β=100.22(2)°   γ=108.10(2)°

C9H17BN2S2

C9H17BN2S2

Liu, SiyuanLégaré, Marc-AndréHofmann, AlexanderBraunschweig, Holger

Journal of the American Chemical Society (2018) 140, 36 11223-11226

a=6.4382(20)Å   b=9.070(3)Å   c=10.891(3)Å

α=75.737(8)°   β=77.099(8)°   γ=74.734(19)°

C9H17BN2Se

C9H17BN2Se

Liu, SiyuanLégaré, Marc-AndréHofmann, AlexanderBraunschweig, Holger

Journal of the American Chemical Society (2018) 140, 36 11223-11226

a=12.404(7)Å   b=7.679(4)Å   c=12.800(7)Å

α=90°   β=108.23(4)°   γ=90°

C9H17BN2S

C9H17BN2S

Liu, SiyuanLégaré, Marc-AndréHofmann, AlexanderBraunschweig, Holger

Journal of the American Chemical Society (2018) 140, 36 11223-11226

a=12.364(3)Å   b=7.522(3)Å   c=12.850(3)Å

α=90°   β=109.438(10)°   γ=90°

C9H17BN2Se2

C9H17BN2Se2

Liu, SiyuanLégaré, Marc-AndréHofmann, AlexanderBraunschweig, Holger

Journal of the American Chemical Society (2018) 140, 36 11223-11226

a=6.587(2)Å   b=9.123(3)Å   c=11.052(4)Å

α=76.48(3)°   β=77.86(3)°   γ=74.261(19)°

C16H22BMnN2O2Te2

C16H22BMnN2O2Te2

Liu, SiyuanLégaré, Marc-AndréHofmann, AlexanderBraunschweig, Holger

Journal of the American Chemical Society (2018) 140, 36 11223-11226

a=9.0510(13)Å   b=9.9167(12)Å   c=21.724(4)Å

α=90°   β=90.139(7)°   γ=90°

C7H13Cl2N3OPt

C7H13Cl2N3OPt

Andreas HofmannDeogratius JaganyiOrde Q. MunroGünter LiehrRudi van Eldik

Inorganic Chemistry (2003) 42, 1688-1700

a=7.073(5)Å   b=8.747(5)Å   c=9.812(5)Å

α=73.28(2)°   β=81.50(2)°   γ=78.10(2)°

Chloro[6-(ortho-phenylene)-2,2-bipyridine-κC,κN,κN]platinum(II) yellow modification

C16H11Cl1N2Pt1

Andreas HofmannLutz DahlenburgRudi van Eldik

Inorganic Chemistry (2003) 42, 6528-6538

a=9.2670(10)Å   b=7.5410(10)Å   c=19.638(2)Å

α=90°   β=99.840(10)°   γ=90°

Chloro[6-(ortho-phenylene)-2,2-bipyridine-κC,κN,κN]platinum(II) red modification

C16H11Cl1N2Pt1

Andreas HofmannLutz DahlenburgRudi van Eldik

Inorganic Chemistry (2003) 42, 6528-6538

a=8.880(5)Å   b=12.336(5)Å   c=13.624(3)Å

α=102.10(3)°   β=102.13(3)°   γ=104.07(4)°

C20H27NO5S

C20H27NO5S

Liepa, A. J.Hofmann, A.Tiekink, E. R. T.

Zeitschrift für Kristallographie - New Crystal Structures (2002) 217, 1 89-90

a=12.262(2)Å   b=12.391(1)Å   c=14.550(1)Å

α=90°   β=113.96(1)°   γ=90°

Sr In2 S4

In2S4Sr

Eisenmann, B.Hofmann, A.

Zeitschrift fuer Kristallographie (149,1979-) (1991) 197, 167-168

a=20.901Å   b=21.12Å   c=13.02Å

α=90°   β=90°   γ=90°

Na7 In3 Se8

In3Na7Se8

Eisenmann, B.Hofmann, A.

Zeitschrift fuer Kristallographie (149,1979-) (1991) 197, 159-160

a=13.506Å   b=6.747Å   c=10.438Å

α=90.159°   β=91.243°   γ=90.003°

Ca0.76In2.84S5

Ca0.76In2.84S5

Eisenmann, B.Hofmann, A.

Zeitschrift fuer Kristallographie (149,1979-) (1991) 197, 165-166

a=15.988Å   b=12.619Å   c=3.843Å

α=90°   β=90°   γ=90°

K5 Ga Se4

GaK5Se4

Eisenmann, B.Hofmann, A.

Zeitschrift fuer Kristallographie (149,1979-) (1991) 197, 163-164

a=15.665Å   b=12.588Å   c=12.899Å

α=90°   β=90°   γ=90°

K (In S2)

InKS2

Eisenmann, B.Hofmann, A.

Zeitschrift fuer Kristallographie (149,1979-) (1991) 195, 318-319

a=11.003Å   b=10.995Å   c=15.021Å

α=90°   β=100.6°   γ=90°

Na (Al Se2)

AlNaSe2

Eisenmann, B.Hofmann, A.

Zeitschrift fuer Kristallographie (149,1979-) (1991) 197, 171-172

a=10.72Å   b=10.708Å   c=14.126Å

α=90°   β=100.9°   γ=90°

Na6 Al2 Te6

Al2Na6Te6

Eisenmann, B.Hofmann, A.

Zeitschrift fuer Kristallographie (149,1979-) (1991) 197, 139-140

a=8.062Å   b=7.756Å   c=14.106Å

α=90°   β=90.368°   γ=90°

Na6 Al2 Se6

Al2Na6Se6

Eisenmann, B.Hofmann, A.

Zeitschrift fuer Kristallographie (149,1979-) (1991) 197, 141-142

a=7.499Å   b=7.203Å   c=13.196Å

α=90°   β=90.372°   γ=90°

Na6 (S2 (In S2)2)

In2Na6S6

Eisenmann, B.Hofmann, A.

Zeitschrift fuer Kristallographie (149,1979-) (1991) 197, 151-152

a=15.945Å   b=13.456Å   c=7.358Å

α=90°   β=117.406°   γ=90°

Na6 Al2 S6

Al2Na6S6

Eisenmann, B.Hofmann, A.

Zeitschrift fuer Kristallographie (149,1979-) (1991) 197, 161-162

a=13.706Å   b=12.071Å   c=7.608Å

α=90°   β=98.6°   γ=90°

Na6 Ga2 S6

Ga2Na6S6

Eisenmann, B.Hofmann, A.

Zeitschrift fuer Kristallographie (149,1979-) (1991) 197, 147-148

a=13.691Å   b=12.099Å   c=7.653Å

α=90°   β=98.384°   γ=90°

7-I

C10H28I4P4Pt2,C6H6

Brunecker, CarinaArrowsmith, MerleMuessig, JonasBöhnke, JulianStoy, AndreasHeß, MerlinHofmann, AlexanderLenczyk, CarstenLichtenberg, CrispinRempel, AnnaRamler, JacquelineBraunschweig, Holger

Dalton Transactions (2021)

a=8.4725(18)Å   b=8.5638(18)Å   c=10.4628(13)Å

α=111.406(12)°   β=90.373(7)°   γ=92.437(8)°

1

C15H42P6Pt2

Brunecker, CarinaArrowsmith, MerleMuessig, JonasBöhnke, JulianStoy, AndreasHeß, MerlinHofmann, AlexanderLenczyk, CarstenLichtenberg, CrispinRempel, AnnaRamler, JacquelineBraunschweig, Holger

Dalton Transactions (2021)

a=16.4148(5)Å   b=9.8279(4)Å   c=16.8925(7)Å

α=90°   β=104.453(2)°   γ=90°

6-I

C10H28I2P4Pt2

Brunecker, CarinaArrowsmith, MerleMuessig, JonasBöhnke, JulianStoy, AndreasHeß, MerlinHofmann, AlexanderLenczyk, CarstenLichtenberg, CrispinRempel, AnnaRamler, JacquelineBraunschweig, Holger

Dalton Transactions (2021)

a=16.063(5)Å   b=8.568(2)Å   c=15.827(3)Å

α=90°   β=102.115(14)°   γ=90°

4-Cl(NPh2)

C22H38BCl2NP4Pt2,0.5(C6H4F2)

Brunecker, CarinaArrowsmith, MerleMuessig, JonasBöhnke, JulianStoy, AndreasHeß, MerlinHofmann, AlexanderLenczyk, CarstenLichtenberg, CrispinRempel, AnnaRamler, JacquelineBraunschweig, Holger

Dalton Transactions (2021)

a=15.0000(5)Å   b=11.3002(4)Å   c=19.1129(6)Å

α=90°   β=93.1650(10)°   γ=90°

4-Cl(Cl)

C10H28BCl3P4Pt2,0.5(C6H4F2)

Brunecker, CarinaArrowsmith, MerleMuessig, JonasBöhnke, JulianStoy, AndreasHeß, MerlinHofmann, AlexanderLenczyk, CarstenLichtenberg, CrispinRempel, AnnaRamler, JacquelineBraunschweig, Holger

Dalton Transactions (2021)

a=14.055(2)Å   b=11.8205(14)Å   c=15.0133(16)Å

α=90°   β=98.271(9)°   γ=90°

4-Br(Cy)

C16H39BBr2P4Pt2,CH2Cl2

Brunecker, CarinaArrowsmith, MerleMuessig, JonasBöhnke, JulianStoy, AndreasHeß, MerlinHofmann, AlexanderLenczyk, CarstenLichtenberg, CrispinRempel, AnnaRamler, JacquelineBraunschweig, Holger

Dalton Transactions (2021)

a=15.3302(5)Å   b=10.6045(3)Å   c=20.0669(6)Å

α=90°   β=109.9580(10)°   γ=90°

3

C35H98P14Pt4,0.5(C6H14)

Brunecker, CarinaArrowsmith, MerleMuessig, JonasBöhnke, JulianStoy, AndreasHeß, MerlinHofmann, AlexanderLenczyk, CarstenLichtenberg, CrispinRempel, AnnaRamler, JacquelineBraunschweig, Holger

Dalton Transactions (2021)

a=9.7921(6)Å   b=18.6172(12)Å   c=35.799(2)Å

α=86.460(2)°   β=82.591(2)°   γ=83.964(2)°

Pt6 cluster

C14H40P6Pt3

Brunecker, CarinaArrowsmith, MerleMuessig, JonasBöhnke, JulianStoy, AndreasHeß, MerlinHofmann, AlexanderLenczyk, CarstenLichtenberg, CrispinRempel, AnnaRamler, JacquelineBraunschweig, Holger

Dalton Transactions (2021)

a=9.6196(4)Å   b=11.6672(5)Å   c=12.3195(5)Å

α=111.4220(10)°   β=93.2400(10)°   γ=92.7520(10)°

4-Cl(Dur)

C20H41BCl2P4Pt2,2(C6H4F2)

Brunecker, CarinaArrowsmith, MerleMuessig, JonasBöhnke, JulianStoy, AndreasHeß, MerlinHofmann, AlexanderLenczyk, CarstenLichtenberg, CrispinRempel, AnnaRamler, JacquelineBraunschweig, Holger

Dalton Transactions (2021)

a=11.836(4)Å   b=22.892(8)Å   c=14.199(5)Å

α=90°   β=90°   γ=90°

4-I(I)

C12H32BCl4I3P4Pt2

Brunecker, CarinaArrowsmith, MerleMuessig, JonasBöhnke, JulianStoy, AndreasHeß, MerlinHofmann, AlexanderLenczyk, CarstenLichtenberg, CrispinRempel, AnnaRamler, JacquelineBraunschweig, Holger

Dalton Transactions (2021)

a=14.9329(9)Å   b=15.7221(9)Å   c=26.2447(16)Å

α=90°   β=94.570(2)°   γ=90°